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Effect of the synthesis parameters on the physicochemical properties of NaY Zeolite with faujasite structure

2026-02-05Artigo científico Acesso aberto
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datacite.subject.sdg09:Indústria, Inovação e Infraestruturas
datacite.subject.sdg12:Produção e Consumo Sustentáveis
datacite.subject.sdg13:Ação Climática
dc.contributor.authorFernandes, Auguste
dc.contributor.authorPlateau, Christiaan
dc.contributor.authorLourenço, João P.
dc.contributor.authorCosta, Daniel
dc.contributor.authorEsteves, Laura M.
dc.contributor.authorFerreira, Maria João
dc.contributor.authorNogueira, Isabel
dc.contributor.authorRibeiro, Maria Filipa
dc.date.accessioned2026-03-24T13:53:01Z
dc.date.available2026-03-24T13:53:01Z
dc.date.issued2026-02-05en_US
dc.date.updated2026-03-24T13:13:12Z
dc.description.abstractNaY material belongs to the iconic family of zeolites with a Faujasite structure. These microporous aluminosilicate materials possess exceptional properties, making them essential in various applications, e.g., catalysis, gas sorption/separation, and ion exchange. In particular, NaY zeolite is a good model material for teaching fundamental concepts in crystallography, surface chemistry, and adsorption phenomena and a stimulating literature review topic for students. NaY zeolite can be easily synthesized by students at the laboratory scale. Its preparation and characterization offer valuable learning opportunities by linking theoretical knowledge with practical applications in Materials Science and/or Chemical Engineering courses. In this work, we propose a very simple but highly reproducible synthesis method for obtaining a highly crystalline NaY material. This flexible approach enables undergraduate students to investigate the influence of both the crystallization time and temperature on the outcome of NaY synthesis. By combining standard characterization techniques like powder X-ray diffraction, solid-state nuclear magnetic resonance, infrared spectroscopy, and scanning electron microscopy coupled with energy-dispersive spectroscopy, students acquire hands-on experience in Materials characterization, learn about the complementarity and limitations of the different characterization methods, and strengthen their knowledge in Inorganic Chemistry, Materials Science, and Analytical Chemistry.eng
dc.description.sponsorshipPhD grant 2022.11605.BD and contracts 2023.15700.TENURE.041 and 2023.15700.TENURE.029.
dc.description.versioninfo:eu-repo/semantics/publishedVersion
dc.identifier.doi10.1021/acs.jchemed.5c00851en_US
dc.identifier.eissn1938-1328
dc.identifier.issn0021-9584
dc.identifier.slugcv-prod-4713379
dc.identifier.urihttp://hdl.handle.net/10400.1/28525
dc.language.isoeng
dc.peerreviewedyes
dc.publisherAmerican Chemical Society
dc.relationCentro de Química Estrutural
dc.relationCentro de Química Estrutural
dc.rights.urihttp://creativecommons.org/licenses/by/4.0/
dc.subjectUpper-division undergraduate
dc.subjectInorganic chemistry
dc.subjectLaboratory instructions
dc.subjectHands-On learning/manipulatives
dc.subjectMaterials science
dc.subjectChemical Engineering
dc.subjectSolid state chemistry
dc.subjectAtomic spectroscopy
dc.subjectInfrared and NMR
dc.subjectSpectroscopies
dc.subjectX-ray crystallography
dc.titleEffect of the synthesis parameters on the physicochemical properties of NaY Zeolite with faujasite structureeng
dc.typejournal article
dspace.entity.typePublication
oaire.awardNumberUIDB/00100/2020
oaire.awardNumberUIDP/00100/2020
oaire.awardTitleCentro de Química Estrutural
oaire.awardTitleCentro de Química Estrutural
oaire.awardURIinfo:eu-repo/grantAgreement/FCT/6817 - DCRRNI ID/UIDB%2F00100%2F2020/PT
oaire.awardURIinfo:eu-repo/grantAgreement/FCT/6817 - DCRRNI ID/UIDP%2F00100%2F2020/PT
oaire.citation.endPage1479
oaire.citation.issue3en_US
oaire.citation.startPage1472
oaire.citation.titleJournal of Chemical Educationen_US
oaire.citation.volume103en_US
oaire.fundingStream6817 - DCRRNI ID
oaire.fundingStream6817 - DCRRNI ID
oaire.versionhttp://purl.org/coar/version/c_970fb48d4fbd8a85
person.familyNameLourenço
person.givenNameJoão P.
person.identifier634248
person.identifier.ciencia-idF81F-A1F0-2A7C
person.identifier.orcid0000-0002-0501-6672
person.identifier.ridA-7758-2008
person.identifier.scopus-author-id57195730600
project.funder.identifierhttp://doi.org/10.13039/501100001871
project.funder.identifierhttp://doi.org/10.13039/501100001871
project.funder.nameFundação para a Ciência e a Tecnologia
project.funder.nameFundação para a Ciência e a Tecnologia
rcaap.cv.cienciaidF81F-A1F0-2A7C | João Paulo Gil Lourenço
rcaap.rightsopenAccessen_US
relation.isAuthorOfPublicationf66ab886-d989-4c1d-9550-527507723c26
relation.isAuthorOfPublication.latestForDiscoveryf66ab886-d989-4c1d-9550-527507723c26
relation.isProjectOfPublicationdf39fd72-bd68-4aaf-8b89-25d17b8c5ebd
relation.isProjectOfPublication36364d2a-b4fe-4b0f-a8c8-ca575b121cf4
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